(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

Base Information

Chemical Name:(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate
CAS No.:1228104-27-5
Molecular Formula:C₃₁H₄₆Cl₂O₃Si
Molecular Weight:565.696
Hs Code.:

Synonyms:(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

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Technology Process of (2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

There total 1 articles about (2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1228104-24-2
[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate

: 1228104-27-5
(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

Guidance literature:: With N-chloro-succinimide; triphenylphosphine; In toluene; at 20 - 90 ℃;
DOI:10.1021/jo100534d

Reference yield: 95.0%

: 1228104-27-5
(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

: 1228104-22-0
(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecan-1-ol

Guidance literature:: (2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.333333h;

With ammonium chloride; In hexane; dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo100534d