[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate

Base Information

• Chemical Name: [(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate
• CAS No.: 1228104-24-2
• Molecular Formula: C₃₁H₄₆O₄Si
• Molecular Weight: 510.789

Synonyms:[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate

Chemical Property of [(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate

Chemical Property:

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Technology Process of [(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate

There total 1 articles about [(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methanol (1228104-25-3) + pivaloyl chloride (3282-30-2) → [(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate (1228104-24-2)

Guidance literature:

[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methanol; pivaloyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 2.5h;

With dmap; In dichloromethane; for 0.5h;

DOI:10.1021/jo100534d

Reference yield: 85.0%

[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methyl 2,2-dimethylpropanoate (1228104-24-2) → (2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate (1228104-27-5)

Guidance literature:

With N-chloro-succinimide; triphenylphosphine; In toluene; at 20 - 90 ℃;

DOI:10.1021/jo100534d

upstream raw materials:

[(2S,3S)-3-[7-[(tert-butyldiphenylsilyl)oxy]heptyl]oxiran-2-yl]methanol

pivaloyl chloride

Downstream raw materials:

(2R,3R)-10-[(tert-butyldiphenylsilyl)oxy]-2,3-dichlorodecyl 2,2-dimethylpropanoate

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