C₁₈H₂₄O₄

Base Information

Chemical Name:C₁₈H₂₄O₄
CAS No.:1325710-84-6
Molecular Formula:C₁₈H₂₄O₄
Molecular Weight:304.386
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>4</sub>

Synonyms:C₁₈H₂₄O₄

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Chemical Property of C₁₈H₂₄O₄

Chemical Property:

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Technology Process of C₁₈H₂₄O₄

There total 4 articles about C₁₈H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₂O₅

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1325710-84-6
C₁₈H₂₄O₄

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

C₁₇H₂₂O₅; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol201920j

Reference yield:

: 913066-81-6
[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

: 1325710-84-6
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 2 h / pH 7 / Inert atmosphere; aq. buffer

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; potassium tert-butylate; sodium hydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; mineral oil; 3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1021/ol201920j

Reference yield:

: 1325711-08-7
C₂₄H₂₈O₄

: 1325710-84-6
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 2 h / pH 7 / Inert atmosphere; aq. buffer

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; potassium tert-butylate; In tetrahydrofuran; water; 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1021/ol201920j