diphenyltriethoxyphosphorane

Base Information

• Chemical Name: diphenyltriethoxyphosphorane
• CAS No.: 23855-81-4
• Molecular Formula: C₁₈H₂₅O₃P
• Molecular Weight: 320.368

Synonyms:diphenyltriethoxyphosphorane

Chemical Property of diphenyltriethoxyphosphorane

Chemical Property:

Purity/Quality:

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Technology Process of diphenyltriethoxyphosphorane

There total 3 articles about diphenyltriethoxyphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl peroxide (628-37-5) + (2-cyanoethyl)diphenylphosphine (5032-65-5) → Ethyl diphenylphosphinite (719-80-2) + diethyl ether (60-29-7,927820-24-4) + 3-(diphenylphosphinyl)propanenitrile (5032-67-7) + diphenyltriethoxyphosphorane (23855-81-4) + acrylonitrile (107-13-1,25014-41-9) + C17H18NOP

Guidance literature:

In benzene-d6; for 72h; Product distribution; Ambient temperature; in a sealed tube;

Reference yield:

Ethyl diphenylphosphinite (719-80-2) + diethyl peroxide (628-37-5) → diphenyltriethoxyphosphorane (23855-81-4)

Guidance literature:

In dichloromethane;

DOI:10.1021/ja01047a011

Reference yield:

diethyl peroxide (628-37-5) + isopropyl diphenylphosphinite (27350-46-5) → ethyl diphenylphosphinate (1733-55-7) + isopropyl diphenylphosphinate (1706-91-8) + diphenyltriethoxyphosphorane (23855-81-4) + C19H27O3P

Guidance literature:

In benzene; at 35 ℃; for 504h; Product distribution; further diarylphosphinites;

upstream raw materials:

Ethyl diphenylphosphinite

diethyl peroxide

(2-cyanoethyl)diphenylphosphine

isopropyl diphenylphosphinite

Downstream raw materials:

(8-TB-5-11)-8,8-diphenyl-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

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