Technology Process of C35H40N2O3S
There total 11 articles about C35H40N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Lawessons reagent;
In
toluene;
at 110 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C / Inert atmosphere
2: lithium hydroxide; water / methanol; tetrahydrofuran / 16 h / Heating
3: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 1 h / 20 °C / Cooling with ice
4: triethylamine / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
5: Lawessons reagent / toluene / 3 h / 110 °C
With
Lawessons reagent; oxalyl dichloride; water; potassium carbonate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium hydroxide; water / methanol; tetrahydrofuran / 16 h / Heating
2: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 1 h / 20 °C / Cooling with ice
3: triethylamine / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
4: Lawessons reagent / toluene / 3 h / 110 °C
With
Lawessons reagent; oxalyl dichloride; water; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;