P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

Base Information

Chemical Name:P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester
CAS No.:486429-74-7
Molecular Formula:C₁₁H₁₇PSSe
Molecular Weight:291.256
Hs Code.:

Synonyms:P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

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Chemical Property of P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

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Technology Process of P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

There total 8 articles about P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid N,N,N,N-tetramethylammonium salt

: 74-88-4
methyl iodide

: 486429-74-7
P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jo050576c

Reference yield: 91.0%

: P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid N,N,N,N-tetrabutylammonium salt

: 74-88-4
methyl iodide

: 486429-74-7
P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1246/cl.2002.914 DOI:10.1021/jo050576c

Reference yield:

: 29949-69-7,146387-73-7,146387-74-8
tert-butylchlorophenylphosphane

: 486429-74-7
P-(1,1-dimethylethyl)-P-phenylphosphinoselenothioic acid Se-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Se / toluene / 1 h / Heating

2: Na₂S / acetonitrile / 6 h / 20 °C

3: 0.261 g / acetonitrile / 1 h / 20 °C

With sodium sulfide; selenium; In toluene; acetonitrile;
DOI:10.1021/jo0484979