2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

Base Information

Chemical Name:2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene
CAS No.:196403-57-3
Molecular Formula:C₁₅H₁₈F₃NO₂
Molecular Weight:301.309
Hs Code.:

Synonyms:2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

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Chemical Property of 2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

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Technology Process of 2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

There total 1 articles about 2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 116233-18-2
2-Bromo-3-nitro-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

: 196403-57-3
2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

Guidance literature:: With copper(l) iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1016/S0960-894X(97)00382-X

Reference yield:

: 196403-57-3
2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

: 245369-52-2
Methyl 4-[1-(5,6,7,8-tetrahydro-3-trifluoromethyl-5,5,8,8-tetramethyl-2-naphthalenyl)carbamoyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Fe; HCl; H₂O / various solvent(s) / Heating

2: 96 percent / pyridine / benzene / 20 °C

With pyridine; hydrogenchloride; water; iron; In benzene; 1: Reduction / 2: Condensation;
DOI:10.1016/S0022-1139(99)00070-6

Reference yield:

: 196403-57-3
2-Nitro-3-trifluoromethyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene

: 4-[1-(5,6,7,8-Tetrahydro-3-trifluoromethyl-5,5,8,8-tetramethyl-2-naphthalenyl)carbamoyl]benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Fe; HCl; H₂O / various solvent(s) / Heating

2: 96 percent / pyridine / benzene / 20 °C

3: 95 percent / NaOH; H₂O / ethanol / Heating

With pyridine; hydrogenchloride; sodium hydroxide; water; iron; In ethanol; benzene; 1: Reduction / 2: Condensation / 3: Hydrolysis;
DOI:10.1016/S0022-1139(99)00070-6