Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

Base Information

Chemical Name:Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester
CAS No.:872692-55-2
Molecular Formula:C₂₁H₂₂N₄O₅
Molecular Weight:410.429
Hs Code.:

Synonyms:Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

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Chemical Property of Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

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Technology Process of Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

There total 2 articles about Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 924-44-7
glyoxylic acid ethyl ester

: 855594-74-0
(4S)-4-((4'-methoxyphenyl)methyl)-2-oxazolidinone

: 872692-55-2
Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;
DOI:10.1055/s-2005-918925 DOI:10.3987/com-06-s(k)41

Reference yield:

: 126395-29-7
[(S)-2-hydroxy-1-(4-methoxybenzyl)ethyl]carbamic acid tert-butyl ester

: 872692-55-2
Benzotriazol-1-yl-[(S)-4-(4-methoxy-benzyl)-2-oxo-oxazolidin-3-yl]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaH / tetrahydrofuran / Heating

2: 84 percent / PTSA / toluene / Heating

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1055/s-2005-918925