4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Base Information

Chemical Name:4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)
CAS No.:1322745-46-9
Molecular Formula:C₂₂H₁₉Cl₂N₃O₃
Molecular Weight:444.317
Hs Code.:

Synonyms:4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Suppliers and Price of 4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

There total 4 articles about 4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1322745-45-8
5-cyano-4-(4-methoxyphenyl)-6-methylpyridine-2-carboxylic acid

: 1322745-46-9
4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Guidance literature:: With hydroxylamine hydrochloride; potassium tert-butylate; In dimethyl sulfoxide; at 100 ℃; for 16h;
DOI:10.1002/jhet.614

Reference yield:

: 1253518-31-8
5-cyano-4-(4-methoxyphenyl)-6-methylpyridine-2-carboxylic acid

: 1322745-46-9
4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / dichloromethane / 3 h / 20 °C

2: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide / 16 h / 100 °C

With hydroxylamine hydrochloride; potassium tert-butylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/jhet.614

Reference yield:

: 17451-21-7,128935-12-6
(E)-4-(4-methoxy-phenyl)-2-oxo-3-butenoic acid

: 1322745-46-9
4-(4-methoxyphenyl)-6-methyl-pyridine-2,5-dicarboxylic acid 5-amide 2-(3,4-dichlorobenzylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / 16 h / 20 °C

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / dichloromethane / 3 h / 20 °C

3: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide / 16 h / 100 °C

With hydroxylamine hydrochloride; potassium tert-butylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/jhet.614