2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Base Information

• Chemical Name: 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone
• CAS No.: 69530-90-1
• Molecular Formula: C₂₄H₄₂N₂O₄S
• Molecular Weight: 454.674

Synonyms:2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Chemical Property of 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Chemical Property:

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Technology Process of 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

There total 8 articles about 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

acetone (67-64-1) + (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-51-1) → (Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-52-2) + 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (69530-90-1)

Guidance literature:

With n-butyllithium; In 1,2-dimethoxyethane; at -65 ℃; for 0.333333h; Yield given;

DOI:10.1039/P19810002848

Reference yield: 31.0%

acetone-2,4,6-tri-isopropylbenzenesulphonylhydrazone (61835-96-9) + acetone (67-64-1) → (Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-52-2) + 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (69530-90-1) + (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-51-1)

Guidance literature:

With n-butyllithium; In 1,2-dimethoxyethane; at -78 ℃; Yield given;

DOI:10.1039/P19810002848

Reference yield: 30.0%

(Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-52-2) + acetone (67-64-1) → 2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (69530-90-1) + (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone (80703-51-1)

Guidance literature:

With n-butyllithium; acetic acid; In 1,2-dimethoxyethane; at -65 ℃; for 0.333333h;

DOI:10.1039/P19810002848

upstream raw materials:

acetone-2,4,6-tri-isopropylbenzenesulphonylhydrazone

acetone

(Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

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