(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Base Information

Chemical Name:(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone
CAS No.:80703-51-1
Molecular Formula:C₂₁H₃₆N₂O₃S
Molecular Weight:396.594
Hs Code.:

Synonyms:(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Suppliers and Price of (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Chemical Property:

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Technology Process of (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

There total 6 articles about (E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 61835-96-9
acetone-2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 67-64-1
acetone

: 80703-52-2
(Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 69530-90-1
2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 80703-51-1
(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Guidance literature:: With n-butyllithium; In 1,2-dimethoxyethane; at -78 ℃; Yield given;
DOI:10.1039/P19810002848

Reference yield: 30.0%

: 80703-52-2
(Z)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 67-64-1
acetone

: 69530-90-1
2,6-dihydroxy-2,6-dimethylheptan-4-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 80703-51-1
(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Guidance literature:: With n-butyllithium; acetic acid; In 1,2-dimethoxyethane; at -65 ℃; for 0.333333h;
DOI:10.1039/P19810002848

Reference yield:

: 39085-59-1
trisylhydrazine

: 80703-51-1
(E)-4-hydroxy-4-methylpentan-2-one 2,4,6-tri-isopropylbenzenesulphonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / Heating

2: n-butyl-lithium / 1,2-dimethoxy-ethane / 0.33 h / -65 °C

With n-butyllithium; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1039/P19810002848