Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

Base Information

Chemical Name:Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside
CAS No.:130450-83-8
Molecular Formula:C₆₁H₆₄O₁₁
Molecular Weight:973.173
Hs Code.:

Synonyms:Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

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Chemical Property of Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

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Technology Process of Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

There total 23 articles about Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 130450-81-6
Methyl 2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

: 130450-82-7
Benzyl 4-O-(4-O-acetyl-2,3-di-O-benzyl-α-D-xylopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 130450-86-1
Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-β-D-xylopyranosyl>-β-D-glucopyranoside

: 130450-83-8
Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; methyl trifluoromethanesulfonate; In diethyl ether; 1.)r.t., 30 min., 2.)r.t., 6 h;
DOI:10.1016/0008-6215(90)84242-M

Reference yield: 50.0%

: 67831-42-9
benzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 130450-81-6
Methyl 2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

: 130450-86-1
Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-β-D-xylopyranosyl>-β-D-glucopyranoside

: 130450-83-8
Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; methyl trifluoromethanesulfonate; In diethyl ether; 1.)r.t., 30 min., 2.)r.t., 6 h;
DOI:10.1016/0008-6215(90)84242-M

Reference yield:

: 100-39-0
benzyl bromide

: 130450-83-8
Benzyl 2,3,6-tri-O-benzyl-4-O-<2,3-di-O-benzyl-4-O-(p-methoxybenzyl)-α-D-xylopyranosyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.)NaH / 1.)DMF, 2.)r.t.

2: 50 percent / CuBr₂, Bu₄NBr, molecular sieve 4A / 1,2-dichloro-ethane; dimethylformamide / 72 h / Ambient temperature

With 4 A molecular sieve; tetrabutylammomium bromide; sodium hydride; copper(ll) bromide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M