2-methyl-5-(p-nitrophenyl)furan

Base Information

Chemical Name:2-methyl-5-(p-nitrophenyl)furan
CAS No.:60456-78-2
Molecular Formula:C₁₁H₉NO₃
Molecular Weight:203.197
Hs Code.:

Synonyms:2-methyl-5-(p-nitrophenyl)furan

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Chemical Property of 2-methyl-5-(p-nitrophenyl)furan

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Technology Process of 2-methyl-5-(p-nitrophenyl)furan

There total 9 articles about 2-methyl-5-(p-nitrophenyl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 534-22-5
2-methylfuran

: 586-78-7
para-nitrophenyl bromide

: 60456-78-2
2-methyl-5-(p-nitrophenyl)furan

Guidance literature:: With [Pd(IPr*IMe)^An(3-Cl-pyridinyl)Cl₂]; potassium carbonate; acetic acid; In N,N-dimethyl acetamide; at 130 ℃; for 12h; Reagent/catalyst; Solvent; regioselective reaction; Catalytic behavior;
DOI:10.1021/acs.organomet.0c00494

Reference yield: 95.0%

: 636-98-6
p-nitrobenzene iodide

: 35523-16-1
bis(5-methyl-2-furyl)mercury

: 60456-78-2
2-methyl-5-(p-nitrophenyl)furan

Guidance literature:: With sodium iodide; (4-nitrophenyl)Pd(P(C₆H₅)3)2I; In N,N-dimethyl-formamide; cross-coupling react. of the corresponding (A)2Hg with the corresponding ArI in DMF in the presence of NaI and the Pd catalyst under Ar (20°C, 10 min);
DOI:10.1016/0022-328X(89)85346-X