9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

Base Information

Chemical Name:9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate
CAS No.:272107-48-9
Molecular Formula:CF₃O₃S*C₂₃H₂₀NO₂
Molecular Weight:491.488
Hs Code.:

Synonyms:9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

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Chemical Property of 9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

There total 4 articles about 9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 216668-66-5
2,6-dimethylphenyl acridine-9-carboxylate

: 333-27-7
methyl trifluoromethanesulfonate

: 272107-48-9
9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo1020882

Reference yield:

: 5336-90-3
acridine-9-carboxylic acid

: 272107-48-9
9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: dmap; triethylamine / dichloromethane / 20 °C

3: dichloromethane / 20 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo1020882

Reference yield:

: 66074-67-7
9-acridinecarbonyl chloride

: 272107-48-9
9-[(2,6-dimethylphenoxy)carbonyl]-10-methylacridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: 2,6-di-tert-butyl-pyridine / dichloromethane / 20 °C

With dmap; 2,6-di-tert-butyl-pyridine; triethylamine; In dichloromethane;
DOI:10.1016/j.saa.2010.10.029