1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

Base Information

Chemical Name:1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline
CAS No.:1417305-21-5
Molecular Formula:C₁₇H₁₂BF₂NO
Molecular Weight:295.096
Hs Code.:

1,1-difluoro-3-phenyl-1H-1λ<sup>4</sup>,11λ<sup>4</sup>-[1,3,2]oxazaborinino[3,4-a]quinoline

Synonyms:1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

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Chemical Property of 1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

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Technology Process of 1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

There total 7 articles about 1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 109-63-7
boron trifluoride diethyl etherate

: 1417305-21-5
1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

Guidance literature:: 1-phenyl-2-(quinolin-2-yl)ethanol; With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.jorganchem.2013.06.012

Reference yield: 82.0%

: 1531-38-0
2-benzoylmethylquinoline

: 109-63-7
boron trifluoride diethyl etherate

: 1417305-21-5
1,1-difluoro-3-phenyl-1H-1λ⁴,11λ⁴-[1,3,2]oxazaborinino[3,4-a]quinoline

Guidance literature:: With n-butyllithium; In hexane; toluene; at -70 ℃; for 1h; Schlenk technique; Inert atmosphere; Reflux;
DOI:10.1016/j.ica.2013.05.034