mesityl(2-methyl-o-carbaboran-1-yl)methanol

Base Information

Chemical Name:mesityl(2-methyl-o-carbaboran-1-yl)methanol
CAS No.:86012-57-9
Molecular Formula:C₁₃H₂₆B₁₀O
Molecular Weight:306.459
Hs Code.:

Synonyms:mesityl(2-methyl-o-carbaboran-1-yl)methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mesityl(2-methyl-o-carbaboran-1-yl)methanol

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Technology Process of mesityl(2-methyl-o-carbaboran-1-yl)methanol

There total 5 articles about mesityl(2-methyl-o-carbaboran-1-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 86012-56-8
mesityl 2-methyl-o-carbaboran-1-yl ketone

: 34557-54-5,27936-85-2
methane

: 74-84-0
ethane

: 86012-57-9
mesityl(2-methyl-o-carbaboran-1-yl)methanol

Guidance literature:: With hydrogenchloride; methylmagnesium chloride; In tetrahydrofuran; soln. of CH3MgCl added to soln. of ketone heated to the boil; boiled (3h); decompd. with aq. HCl; extd. (ether); dried (MgSO4); ether removed; residue ground (pentane, 20°C); filtered off; crystd. (hot hexane); residue recrystd. (toluene);

Reference yield: 93.0%

: 86012-56-8
mesityl 2-methyl-o-carbaboran-1-yl ketone

: 6921-34-2
benzylmagnesium chloride

: 86012-57-9
mesityl(2-methyl-o-carbaboran-1-yl)methanol

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; diethyl ether; soln. of (C6H5)CH2MgCl in ether added to soln. of ketone in THF; heatedto 40°C; boiled (4 h); cooled; decompd. with aq. HCl; org. layer sepd.; dried (CaCl2); solvent removed (vac.); residue extd. (20°C, pentane); recrystd. (toluene);

Reference yield: 93.0%

: 86012-56-8
mesityl 2-methyl-o-carbaboran-1-yl ketone

: 92-52-4,1594-86-1
biphenyl

: 86012-57-9
mesityl(2-methyl-o-carbaboran-1-yl)methanol

Guidance literature:: With hydrogenchloride; phenylmagnesium bromide; In tetrahydrofuran; soln. of C6H5MgBr added to soln. of ketone; boiled (4 h); cooled; decompd. with aq. HCl; extd. (ether); dried (MgSO4); ether removed; residue ground (pentane, 20°C); filtered off; residue sepd. by fractional crystd. (hot hexane); residue recrystd. (toluene);