((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

Base Information

Chemical Name:((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane
CAS No.:165961-03-5
Molecular Formula:C₂₇H₅₀O₅SSi
Molecular Weight:514.842
Hs Code.:

Synonyms:((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

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Technology Process of ((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

There total 7 articles about ((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 165961-02-4
tert-Butyl-((R)-4-methoxymethoxy-13-phenylsulfanyl-tridecyloxy)-dimethyl-silane

: 165961-03-5
((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

Guidance literature:: With magnesium monoperoxyphthalate hexahydrate; In ethanol; for 12h; Ambient temperature;
DOI:10.1021/jo00119a019

Reference yield:

: 165961-00-2
(R)-13-(tert-Butyl-dimethyl-silanyloxy)-10-methoxymethoxy-tridecan-1-ol

: 165961-03-5
((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / pyridine / 41 h / -20 °C

2: 92 percent / NaH / tetrahydrofuran / 1.) 30 min, 2.) room temp., 2 h

3: 95 percent / aq. magnesium monoperoxyphthalate / ethanol / 12 h / Ambient temperature

With pyridine; sodium hydride; magnesium monoperoxyphthalate hexahydrate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo00119a019

Reference yield:

: 165960-98-5
(R)-13-Benzyloxy-4-methoxymethoxy-tridecan-1-ol

: 165961-03-5
((R)-13-Benzenesulfonyl-4-methoxymethoxy-tridecyloxy)-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / Et₃N, imidazole / CH₂Cl₂ / 18 h / Ambient temperature

2: 99 percent / Li, liq. NH₃ / diethyl ether / 1.) -78 deg C, 30 min, 2.) room temp., 3 h

3: 97 percent / pyridine / 41 h / -20 °C

4: 92 percent / NaH / tetrahydrofuran / 1.) 30 min, 2.) room temp., 2 h

5: 95 percent / aq. magnesium monoperoxyphthalate / ethanol / 12 h / Ambient temperature

With pyridine; 1H-imidazole; ammonia; lithium; sodium hydride; magnesium monoperoxyphthalate hexahydrate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo00119a019