2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

Base Information

Chemical Name:2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester
CAS No.:898561-91-6
Molecular Formula:C₄₀H₃₄NO₆P
Molecular Weight:655.687
Hs Code.:

2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

Synonyms:2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

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Chemical Property of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

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Technology Process of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

There total 4 articles about 2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 60254-10-6
(o-hydroxyphenyl)diphenylphosphine

: 144120-53-6
(S)-3-(((9H-fluoren-9-yl)methoxy)carbonylamino)-4-(allyloxy)-4-oxobutanoic acid

: 898561-91-6
2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1021/jo060409s

Reference yield:

: 824-91-9
O-methoxymethylphenol

: 898561-91-6
2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi; TMEDA / hexane / 1.5 h / 20 °C

1.2: 61 percent / hexane / 16 h / 20 °C

2.1: 77 percent / HCl / methanol / 1 h / 20 °C

3.1: 80 percent / N,N-dimethylaminopyridine; N,N'-dicylohexylcarbodiimide / CH₂Cl₂ / 20 h / 20 °C

With hydrogenchloride; dmap; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dicyclohexyl-carbodiimide; In methanol; hexane; dichloromethane;
DOI:10.1021/jo060409s

Reference yield:

: 62815-32-1
methoxymethyl o-diphenylphosphinophenyl ether

: 898561-91-6
2-(9H-fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-allyl ester 4-(2-diphenylphosphanyl-phenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / HCl / methanol / 1 h / 20 °C

2: 80 percent / N,N-dimethylaminopyridine; N,N'-dicylohexylcarbodiimide / CH₂Cl₂ / 20 h / 20 °C

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/jo060409s