2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

Base Information

Chemical Name:2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone
CAS No.:76799-56-9
Molecular Formula:C₄₂H₄₅O₉P
Molecular Weight:724.788
Hs Code.:

Synonyms:2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

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Chemical Property of 2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

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Technology Process of 2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

There total 2 articles about 2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 76799-55-8
2,3',6-tris(benzyloxy)-4-(3-bromopropoxy)-4'-methoxydihydrochalcone

: 121-45-9
phosphorous acid trimethyl ester

: 76799-56-9
2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

Guidance literature:: for 39h; Heating;
DOI:10.1021/jm00136a011

Reference yield:

: 63240-52-8
2,3',6-tris(benzyloxy)-4-hydroxy-4'-methoxydihydrochalcone

: 76799-56-9
2,3',6-tris(benzyloxy)-4-(dimethyl-3-phosphopropyloxy)-4'-methoxydihydrochalcone

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 64 percent / 39 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011