(+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate

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Chemical Name:(+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate
CAS No.:724445-42-5
Molecular Formula:C₂HF₃O₂*C₁₉H₂₃N₃O₄
Molecular Weight:471.433
Hs Code.:

Synonyms:(+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate

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Chemical Property of (+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate

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Technology Process of (+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate

There total 1 articles about (+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 724445-33-4
methyl 3-(benzoyloxy)-9-bromo-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-2-carboxylate

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 2627-86-3
(S)-1-phenyl-ethylamine

: 76-05-1
trifluoroacetic acid

: C₂HF₃O₂*C₁₉H₂₃N₃O₄

: 724445-42-5
(+)-3-hydroxy-2-(methoxycarbonyl)-N-methyl-4-oxo-N-[(1S)-1-phenylethyl]-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-ammonium trifluoroacetate

Guidance literature:: methyl 3-(benzoyloxy)-9-bromo-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-2-carboxylate; (S)-1-phenyl-ethylamine; In methanol; water; at -30 - 20 ℃; for 2.5h;

formaldehyd; With sodium cyanoborohydride; acetic acid; In methanol; water; at 20 ℃; for 0.333333h; pH=5;

trifluoroacetic acid; In water; pH=2 - 3;