[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br

Base Information

• Chemical Name: [CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br
• CAS No.: 1346936-38-6
• Molecular Formula: Br*C₁₈H₂₉BCl₂NO₃
• Molecular Weight: 469.054
• Mol file: 1346936-38-6.mol

Synonyms:[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br

Chemical Property of [CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br

There total 5 articles about [CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]⁽¹⁺⁾*Br^(1-)=[CH₃N(C₂H₄Cl)2CH₂C₆H₄OBO₂C₂(CH₃)4]Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide (1346936-27-3) → (4-hydroxyphenyl)methanol (623-05-2) + [CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4](1+)*Br(1-)=[CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4]Br (1346936-38-6)

Guidance literature:

With dihydrogen peroxide; In water-d2; dimethyl sulfoxide; for 24h; pH=7.5; aq. phosphate buffer;

DOI:10.1021/ja2073824

Reference yield: 5.0%

N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide (1346936-27-3) → [CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4](1+)*Br(1-)=[CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4]Br (1346936-38-6)

Guidance literature:

With dihydrogen peroxide; In water-d2; dimethyl sulfoxide; for 2h; pH=7.5; aq. phosphate buffer;

DOI:10.1021/ja2073824

Reference yield:

4-bromomethylphenylboronic acid pinacol ester (138500-85-3) → (4-hydroxyphenyl)methanol (623-05-2) + [CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4](1+)*Br(1-)=[CH3N(C2H4Cl)2CH2C6H4OBO2C2(CH3)4]Br (1346936-38-6)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 72 h / 20 °C

2: dihydrogen peroxide / water-d2; dimethyl sulfoxide / 24 h / pH 7.5 / aq. phosphate buffer

With dihydrogen peroxide; In dichloromethane; water-d2; dimethyl sulfoxide;

DOI:10.1021/ja2073824

upstream raw materials:

N, N-bis(2-chloroethyl)-N-methyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl] methanaminium bromide

N-Methyldiethanolamine

4-bromomethylphenylboronic acid pinacol ester