(4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide

Base Information

• Chemical Name: (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide
• CAS No.: 107782-99-0
• Molecular Formula: C₂₇H₂₀N₃OP
• Molecular Weight: 433.449
• Mol file: 107782-99-0.mol

Synonyms:(4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide

Chemical Property of (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide

There total 3 articles about (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-chloro-4,6-diphenyl-1,3,5-triazine (3842-55-5) + diphenylphosphane (829-85-6) → (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide (107782-99-0)

Guidance literature:

2-chloro-4,6-diphenyl-1,3,5-triazine; diphenylphosphane; In N,N-dimethyl-formamide; at 110 ℃; for 24h; Inert atmosphere;

With dihydrogen peroxide; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;

DOI:10.1039/d1sc05753g

Reference yield:

bromobenzene (108-86-1,52753-63-6) → (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide (107782-99-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 60 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide; palladium diacetate / 24 h / 130 °C / Inert atmosphere

With iodine; palladium diacetate; magnesium; N,N-dimethyl-formamide; In tetrahydrofuran;

DOI:10.1039/c8tc02010h

Reference yield:

→ (4,6-diphenyl-1,3,5-triazin-2-yl)diphenylphosphine oxide (107782-99-0)

Guidance literature:

2--4.6-diphenyl-1.3.5-triazin (V), O2, Bzl.+A.;

upstream raw materials:

bromobenzene

2-chloro-4,6-diphenyl-1,3,5-triazine

diphenylphosphane