methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

Base Information

• Chemical Name: methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate
• CAS No.: 1448055-17-1
• Molecular Formula: C₃₁H₃₅NO₂
• Molecular Weight: 453.624

Synonyms:methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

Chemical Property of methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

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Technology Process of methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate

There total 2 articles about methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H33NO2 (1448055-13-7) + methyl iodide (74-88-4) → methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate (1448055-17-1)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 16h; diastereoselective reaction; Inert atmosphere;

DOI:10.1039/c4ob00274a

Reference yield:

C30H33NO2 + methyl iodide (74-88-4) → methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate (1448055-17-1) + methyl (2R,3S,1'R,αS,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate (1448055-18-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 16h;

DOI:10.1039/c3cc43250e

Reference yield: 80.0%

methyl (S,S,S,S,E)-2-(1'-phenylprop-2'-en-1'-yl)-3-[N-benzyl-N-(α-methylbenzyl)amino]hex-4-enoate (1448055-17-1) → methyl (S,S,S,S)-2-[N-benzyl-N-(α-methylbenzyl)amino]-5-phenylcyclopent-3-ene-1-carboxylate (1448055-23-9)

Guidance literature:

With Grubbs catalyst first generation; In dichloromethane; at 40 ℃; for 24h;

DOI:10.1039/c3cc43250e

upstream raw materials:

methyl iodide

C₃₀H₃₃NO₂

Downstream raw materials:

methyl (S,S,S,S)-2-[N-benzyl-N-(α-methylbenzyl)amino]-5-phenylcyclopent-3-ene-1-carboxylate

methyl (S,S,S)-2-amino-5-phenylcyclopentane-1-carboxylate

(S,S,S)-2-amino-5-phenylcyclopentane-1-carboxylic acid

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