C₂₇H₃₀ClNOS

Base Information

Chemical Name:C₂₇H₃₀ClNOS
CAS No.:1607800-30-5
Molecular Formula:C₂₇H₃₀ClNOS
Molecular Weight:452.06
Hs Code.:

Synonyms:C₂₇H₃₀ClNOS

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Chemical Property of C₂₇H₃₀ClNOS

Chemical Property:

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Technology Process of C₂₇H₃₀ClNOS

There total 10 articles about C₂₇H₃₀ClNOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1607800-48-5
C₂₆H₂₈ClNOS

: 74-88-4
methyl iodide

: 1607800-30-5
C₂₇H₃₀ClNOS

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.03.012

Reference yield:

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 1607800-30-5
C₂₇H₃₀ClNOS

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfuric acid / 3.5 h / Reflux; Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

3.2: 0.33 h / 20 °C / Inert atmosphere

4.1: toluene / 0.33 h / Inert atmosphere; Reflux

5.1: hydrogen; palladium on activated charcoal / ethanol / 10 h / 20 °C / Inert atmosphere

6.1: hydrogen bromide / acetic acid / 3 h / Inert atmosphere; Reflux

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / N,N-dimethyl-formamide / 8 h / 0 - 20 °C / Inert atmosphere

8.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C / Inert atmosphere

9.1: Lawessons reagent / tetrahydrofuran / 0.25 h / Inert atmosphere; Reflux

10.1: potassium carbonate / acetone / 6 h / 20 °C / Inert atmosphere

With Lawessons reagent; dmap; oxalyl dichloride; sulfuric acid; palladium on activated charcoal; hydrogen bromide; hydrogen; sodium hydride; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetone; toluene; 4.1: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.03.012

Reference yield:

: 15823-04-8
methyl 3-(4-methoxyphenyl)propionate

: 1607800-30-5
C₂₇H₃₀ClNOS

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.33 h / 20 °C / Inert atmosphere

3.1: toluene / 0.33 h / Inert atmosphere; Reflux

4.1: hydrogen; palladium on activated charcoal / ethanol / 10 h / 20 °C / Inert atmosphere

5.1: hydrogen bromide / acetic acid / 3 h / Inert atmosphere; Reflux

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / N,N-dimethyl-formamide / 8 h / 0 - 20 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C / Inert atmosphere

8.1: Lawessons reagent / tetrahydrofuran / 0.25 h / Inert atmosphere; Reflux

9.1: potassium carbonate / acetone / 6 h / 20 °C / Inert atmosphere

With Lawessons reagent; dmap; oxalyl dichloride; palladium on activated charcoal; hydrogen bromide; hydrogen; sodium hydride; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetone; toluene; 3.1: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.03.012