ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

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Chemical Name:ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate
CAS No.:1606993-91-2
Molecular Formula:C₃₉H₆₁NO₄
Molecular Weight:607.918
Hs Code.:

Synonyms:ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

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Chemical Property of ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

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Technology Process of ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

There total 5 articles about ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 623-73-4
diazoacetic acid ethyl ester

: 629-80-1
n-hexadecylaldehyde

: 1072879-54-9
3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine

: 1606993-91-2
ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

Guidance literature:: 3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine; With triphenylborane; In toluene; at 80 ℃; for 0.5h; Inert atmosphere; Sealed tube; Schlenk technique;

diazoacetic acid ethyl ester; n-hexadecylaldehyde; In toluene; stereoselective reaction; Inert atmosphere; Sealed tube; Schlenk technique; Molecular sieve;
DOI:10.1021/acs.orglett.7b00697

Reference yield: 70.0%

: 623-73-4
diazoacetic acid ethyl ester

: 629-80-1
n-hexadecylaldehyde

: 1072879-54-9
3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine

: 1606993-91-2
ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

: C₅₁H₈₅NO₂

: C₃₉H₆₁NO₄

: C₃₉H₆₁NO₄

Guidance literature:: 3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine; With triphenylborane; (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In toluene; at 80 ℃; for 0.5h; Inert atmosphere;

diazoacetic acid ethyl ester; n-hexadecylaldehyde; In toluene; at 0 ℃; for 24h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201301766

Reference yield: 60.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1072879-54-9
3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine

: C₃₅H₅₅NO₂

: 1606993-91-2
ethyl (2S,3S)-1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

: C₅₁H₈₅NO₂

: C₃₉H₆₁NO₄

Guidance literature:: 3,3',5,5'-tetramethyl-4,4'-dimethoxy benzhydrylamine; With triphenylborane; (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In toluene; at 80 ℃; for 0.5h; Inert atmosphere;

diazoacetic acid ethyl ester; C₃₅H₅₅NO₂; In toluene; at 0 ℃; for 24h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201301766