2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

Base Information

Chemical Name:2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane
CAS No.:77084-18-5
Molecular Formula:C₂₂H₂₆O₁₀
Molecular Weight:450.442
Hs Code.:

Synonyms:2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

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Chemical Property of 2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

Chemical Property:

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Technology Process of 2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

There total 5 articles about 2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 131168-59-7
2-(2',4',5'-trimethoxybenzoyloxy)-3,4,5,6-tetramethoxyacetophenone

: 77084-18-5
2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

Guidance literature:: With potassium hydroxide; In pyridine; at 60 ℃; for 4h;

Reference yield:

: 70460-31-0
2',4',5,5',6,7,8-heptamethoxyflavone

: 3162-28-5
2-hydroxy-3,4,5,6-tetramethoxyacetophenone

: 77084-18-5
2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

: 1818-28-6
2',4',5'-trimethoxyacetophenone

Guidance literature:: With potassium hydroxide; In methanol;
DOI:10.1016/S0031-9422(00)91044-6

Reference yield:

: 7507-98-4
1-(2-hydroxy-3,4,6-trimethoxyphenyl)ethanone

: 77084-18-5
2-hydroxy-3,4,5,6-tetramethoxy-2',4',5'-trimethoxydibenzoylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 33.3 percent / potassium persulphate, sodium hydroxide / H₂O

2: 80 percent / methanol; diethyl ether

3: 85 percent / pyridine / 1 h / 100 °C

4: 75 percent / potassium hydroxide / pyridine / 4 h / 60 °C

With pyridine; potassium hydroxide; sodium hydroxide; potassium peroxomonosulphate; In pyridine; methanol; diethyl ether; water;