triethylene glycol monobutyl ether tosylate

Base Information

Chemical Name:triethylene glycol monobutyl ether tosylate
CAS No.:117783-11-6
Molecular Formula:C₁₇H₂₈O₆S
Molecular Weight:360.472
Hs Code.:

Synonyms:triethylene glycol monobutyl ether tosylate

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Chemical Property of triethylene glycol monobutyl ether tosylate

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Technology Process of triethylene glycol monobutyl ether tosylate

There total 1 articles about triethylene glycol monobutyl ether tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 143-22-6,9004-77-7
triethyleneglycol monobutyl ether

: 98-59-9
p-toluenesulfonyl chloride

: 117783-11-6
triethylene glycol monobutyl ether tosylate

Guidance literature:: triethyleneglycol monobutyl ether; p-toluenesulfonyl chloride; With dmap; In dichloromethane; at 20 ℃;

With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo102358d

Reference yield: 59.0%

: 49864-98-4
1,1,3,3,5,5-hexakis(4-(hydroxymethyl)phenoxy)cyclotriphosphazene

: 117783-11-6
triethylene glycol monobutyl ether tosylate

: hexakiscyclophosphazene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 48h; Heating;

Reference yield:

: 117783-11-6
triethylene glycol monobutyl ether tosylate

: 85030-57-5
2-(2-(2-butoxyethoxy)ethoxy)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 18 h / 80 °C

2: hydrazine hydrate / ethanol / 3 h / 76 °C

With hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; 2: Gabriel's dephthaloylation;
DOI:10.1021/jo102358d