(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

Base Information

Chemical Name:(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether
CAS No.:1033126-39-4
Molecular Formula:C₄₂H₅₈O₆Si
Molecular Weight:687.004
Hs Code.:

(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

Synonyms:(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

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Chemical Property of (-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

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Technology Process of (-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

There total 1 articles about (-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1033126-38-3
(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

: 1822-00-0
trimethylsilylmethyllithium

: 1033126-39-4
(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

Guidance literature:: (-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one; trimethylsilylmethyllithium; In toluene; pentane; at -78 - 20 ℃;

With toluene-4-sulfonic acid; In benzene; at 20 ℃; for 4h; Further stages.;
DOI:10.1021/jo8004233

Reference yield: 77.0%

: 1033126-39-4
(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

: 1033126-40-7
C₄₀H₅₄O₆Si

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In benzene; for 4h; Heating;
DOI:10.1021/jo8004233