(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Chemical Name:(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one
CAS No.:1033126-38-3
Molecular Formula:C₄₁H₅₆O₇Si
Molecular Weight:688.977
Hs Code.:

Synonyms:(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Chemical Property of (-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Technology Process of (-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

There total 1 articles about (-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1033126-73-6
C₄₁H₅₈O₇Si

: 1033126-38-3
(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

Guidance literature:: With dipyridinium dichromate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo8004233

Reference yield: 74.0%

: 1033126-38-3
(-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one

: 1822-00-0
trimethylsilylmethyllithium

: 1033126-39-4
(-)-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(4,4-dimethylhepta-1,6-dien-2-yl)cyclobutyl)methyl tert-butyldiphenylsilyl ether

Guidance literature:: (-)-1-((1R,2S,3R)-2-((2-methoxyethoxy)methoxy)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)cyclobutyl)-3,3-dimethylhex-5-en-1-one; trimethylsilylmethyllithium; In toluene; pentane; at -78 - 20 ℃;

With toluene-4-sulfonic acid; In benzene; at 20 ℃; for 4h; Further stages.;
DOI:10.1021/jo8004233