t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

Base Information

Chemical Name:t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate
CAS No.:1292849-59-2
Molecular Formula:C₂₅H₂₅NO₂
Molecular Weight:371.479
Hs Code.:

Synonyms:t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

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Chemical Property of t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

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Technology Process of t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

There total 4 articles about t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1292816-64-8
t-butyl N-(diphenylmethyl)-N-[(2-bromophenyl)methyl]carbamate

: 1292849-59-2
t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

Guidance literature:: With palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In N,N-dimethyl acetamide; at 130 ℃; for 72h; Inert atmosphere;
DOI:10.1039/c0ob00889c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1292849-59-2
t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 0.5 h / 20 °C / Cooling with ice; Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.58 h / 5 - 20 °C / Inert atmosphere

2.2: 20 h / 20 °C / Inert atmosphere

3.1: palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 72 h / 130 °C / Inert atmosphere

With palladium diacetate; sodium hydride; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In ethanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00889c

Reference yield:

: 91-00-9
Benzhydrylamine

: 1292849-59-2
t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 0.5 h / 20 °C / Cooling with ice; Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.58 h / 5 - 20 °C / Inert atmosphere

2.2: 20 h / 20 °C / Inert atmosphere

3.1: palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 72 h / 130 °C / Inert atmosphere

With palladium diacetate; sodium hydride; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In ethanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00889c