6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

Base Information

Chemical Name:6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine
CAS No.:1292849-61-6
Molecular Formula:C₂₀H₁₇N
Molecular Weight:271.362
Hs Code.:

Synonyms:6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

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Chemical Property of 6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

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Technology Process of 6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

There total 4 articles about 6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1292849-59-2
t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate

: 1292849-61-6
6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

Guidance literature:: t-butyl 5-phenyl-5H-dibenz[c,e]azepine-6(7H)-carboxylate; With phosphoric acid; water; In tetrahydrofuran; at 20 ℃; for 72h; Inert atmosphere;

With potassium hydroxide; In tetrahydrofuran; water; at 0 ℃; pH=11; Inert atmosphere;
DOI:10.1039/c0ob00889c

Reference yield:

: 1292816-64-8
t-butyl N-(diphenylmethyl)-N-[(2-bromophenyl)methyl]carbamate

: 1292849-61-6
6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 72 h / 130 °C / Inert atmosphere

2.1: phosphoric acid; water / tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

2.2: 0 °C / pH 11 / Inert atmosphere

With phosphoric acid; water; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1039/c0ob00889c

Reference yield:

: 21420-61-1
N-(tert-butoxycarbonyl)(diphenylmethyl)amine

: 1292849-61-6
6,7-dihydro-5-phenyl-5H-dibenz[c,e]azepine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.58 h / 5 - 20 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 72 h / 130 °C / Inert atmosphere

3.1: phosphoric acid; water / tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

3.2: 0 °C / pH 11 / Inert atmosphere

With phosphoric acid; water; palladium diacetate; sodium hydride; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In tetrahydrofuran; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00889c