2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

Base Information

Chemical Name:2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol
CAS No.:1227408-40-3
Molecular Formula:C₃₉H₄₂N₂O₂
Molecular Weight:570.775
Hs Code.:

Synonyms:2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

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Chemical Property of 2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

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Technology Process of 2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

There total 3 articles about 2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.6%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 223706-42-1
4-methyl-2-tritylphenol

: 108-00-9
N,N-dimethylethylenediamine

: 135-02-4
ortho-anisaldehyde

: 1227408-40-3
2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

Guidance literature:: N,N-dimethylethylenediamine; ortho-anisaldehyde; In ethanol; for 12h;

With sodium tetrahydroborate; ethanol; for 12h;

formaldehyd; 4-methyl-2-tritylphenol; In ethanol; for 12h;

Reference yield: 56.6%

: 626216-36-2
N'-(2-methoxy-benzyl)-N,N-dimethyl-ethylenediamine

: 223706-42-1
4-methyl-2-tritylphenol

: 1227408-40-3
2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

Guidance literature:: With 1,3,5-Trioxan; In ethanol; for 12h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1039/c4dt01122h

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 1227408-40-3
2-{[(2-(dimethylamino)ethyl)(2-methoxybenzyl)amino]methyl}-4-methyl-6-tritylphenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 12 h / Inert atmosphere; Schlenk technique; Reflux

1.2: 12 h / Inert atmosphere; Schlenk technique; Reflux

2.1: 1,3,5-Trioxan / ethanol / 12 h / Inert atmosphere; Schlenk technique; Reflux

With 1,3,5-Trioxan; In ethanol;
DOI:10.1039/c4dt01122h