N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine

Base Information

• Chemical Name: N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine
• CAS No.: 37774-61-1
• Molecular Formula: C₂₈H₁₉N₃
• Molecular Weight: 397.479
• Mol file: 37774-61-1.mol

Synonyms:N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine

Chemical Property of N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine

Chemical Property:

Purity/Quality:

≥99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine

There total 8 articles about N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

N,N-dichloroboryl-[N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl1H-isoindol-1-ylidene)amine] → N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine (37774-61-1)

Guidance literature:

With water; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1039/d0ob00272k

Reference yield: 55.0%

phenylmagnesium bromide (100-58-3) + phthalonitrile (91-15-6) → N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine (37774-61-1)

Guidance literature:

phenylmagnesium bromide; phthalonitrile; In diethyl ether; at -20 - 20 ℃; Inert atmosphere;

With formamide; Reflux;

DOI:10.1002/chem.201002941

Reference yield: 28.0%

phenylmagnesium bromide (100-58-3) + phthalonitrile (91-15-6) → N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine (37774-61-1)

Guidance literature:

In diethyl ether; benzene; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2008.08.026

upstream raw materials:

phenylmagnesium bromide

phthalonitrile

bromobenzene

formamide

Downstream raw materials:

N,N-difluoroboryl-[N-(3-phenyl-2H-isoindol-1-yl)-N-(3-phenyl-1H-isoindol-1-ylidene)amine]

nickel-di-aza-bis-(phenyl)-diisoindolylmethane

zinc-di-aza-bis-(phenyl)-diisoindolylmethane

mercury-di-aza-bis-(phenyl)-diisoindolylmethane