N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Base Information

Chemical Name:N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide
CAS No.:1292804-55-7
Molecular Formula:C₅₁H₇₂N₆O₁₂
Molecular Weight:961.166
Hs Code.:

Synonyms:N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

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Chemical Property of N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

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Technology Process of N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

There total 3 articles about N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1292804-49-9
N'-dodecyl-(2R)-2-(tert-butoxycarbonylamino)-2-[6-deoxy-6-(t-butoxycarbonylamino)-β-D-glucopyranosyl]ethanamide

: 103-71-9
phenyl isocyanate

: 1292804-55-7
N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: With pyridine; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.carres.2011.01.025

Reference yield:

: 1015422-11-3
(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(t-butoxycarbonylamino)-β-D-glucopyranosyl]-ethanoic acid

: 1292804-55-7
N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: Multi-step reaction with 2 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.01.025

Reference yield:

: 124-22-1
n-Dodecylamine

: 1292804-55-7
N'-dodecyl-(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(tert-butoxycarbonylamino-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: Multi-step reaction with 2 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.01.025