N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Base Information

Chemical Name:N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide
CAS No.:1292804-58-0
Molecular Formula:C₆₃H₉₂N₁₀O₁₆
Molecular Weight:1245.48
Hs Code.:

N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Synonyms:N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

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Chemical Property of N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

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Technology Process of N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

There total 6 articles about N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: N'-dodecyl-[[(2R)-2-ammonium-2-]-(6-ammonium-6-deoxy-2,3,4-tri-O-phenylcarbamoyl-)-β-D-glucopyranosyl]ethanamide bistrifluoroacetate

: 207857-15-6
1,3-di(tert-butyloxycarbonyl)-2-(trifluoromethylsulfonyl)guanidine

: 1292804-58-0
N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: With triethylamine; In 1,4-dioxane; water; at 20 ℃; for 12h;
DOI:10.1016/j.carres.2011.01.025

Reference yield:

: 1015422-11-3
(2R)-2-(t-butoxycarbonylamino)-2-[6-deoxy-6-(t-butoxycarbonylamino)-β-D-glucopyranosyl]-ethanoic acid

: 1292804-58-0
N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: Multi-step reaction with 4 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

3: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: triethylamine / 1,4-dioxane; water / 12 h / 20 °C

With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.01.025

Reference yield:

: 124-22-1
n-Dodecylamine

: 1292804-58-0
N'-dodecyl-[[(2R)-2-N,N'-di-t-butoxycarbonyl-guanidinyl-2-]-(6-N,N'-di-t-butoxycarbonyl-guanidinyl-6-deoxy-2,3,4-tri-O-phenylcarbamoyl)-β-D-glucopyranosyl]ethanamide

Guidance literature:: Multi-step reaction with 4 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

3: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: triethylamine / 1,4-dioxane; water / 12 h / 20 °C

With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.01.025