benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate

Base Information

• Chemical Name: benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate
• CAS No.: 1247884-85-0
• Molecular Formula: C₁₄H₁₈N₄O₅S
• Molecular Weight: 354.387
• Mol file: 1247884-85-0.mol

Synonyms:benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate

Chemical Property of benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate

There total 1 articles about benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-azido-3-hydroxypiperidine-1-carboxylic acid benzyl ester (203503-29-1,167832-25-9) + methanesulfonyl chloride (124-63-0) → benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate (1247884-85-0)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield: 62.0%

benzyl 4-azido-3-methanesulfonyloxypiperidine-1-carboxylate (1247884-85-0) → 3,4-diazidopiperidine-1-carboxylic acid benzyl ester (1247884-87-2)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 100 ℃;

upstream raw materials:

4-azido-3-hydroxypiperidine-1-carboxylic acid benzyl ester

methanesulfonyl chloride

Downstream raw materials:

3,4-diazidopiperidine-1-carboxylic acid benzyl ester