bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)

Base Information

Chemical Name:bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)
CAS No.:573701-46-9
Molecular Formula:C₄₈H₆₂P₂Pd
Molecular Weight:807.388
Hs Code.:

Synonyms:bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)

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Chemical Property of bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)

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Technology Process of bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)

There total 1 articles about bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II)

: 247940-06-3
CyJohnPhos

: 573701-46-9
bis(η1-2-(dicyclohexylphosphino)biphenyl)palladium(0)

Guidance literature:: In benzene; byproducts: N,N,N',N'-tetramethylethylenediamine, C2H6; solid mixt. of ligand and Pd complex (molar ratio 2:1) dissolved in benzene; stirred at 55°C for 16 h; volatiles removed in vac.; dissolved in Et2O; crystd. at 0°C; mother liquor removed; crystals washed quickly with cold pentane; dried in vac. for 16 h; elem. anal.;
DOI:10.1021/ja0361493