(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

Base Information

Chemical Name:(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine
CAS No.:74075-28-8
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

Chemical Property:

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Technology Process of (S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

There total 3 articles about (S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74075-27-7
2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<(1S)-1-phthalimido-2-phenylethyl>-1,3-dioxolane

: 74075-28-8
(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

Guidance literature:: With hydrazine; In ethanol; for 0.25h; Heating;
DOI:10.1021/jm00186a020

Reference yield:

: 33861-65-3
N-phthaloyl-L-phenylalanine-2-mercaptopyridyl thioester

: 74075-28-8
(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) magnesium / 1.) THF, from 30 deg C to 35 deg C, 1 h, 2.) THF, RT, 20 h

2: 58 percent / p-toluenesulfonyl chloride / toluene / 11 h

3: 1.3 g / hydrazine / ethanol / 0.25 h / Heating

With magnesium; p-toluenesulfonyl chloride; hydrazine; In ethanol; toluene;
DOI:10.1021/jm00186a020

Reference yield:

: 74075-26-6
2-(3-oxo-5-phenyl-(4S)-4-phthalimidopentyl)-1,3-dioxolane

: 74075-28-8
(S)-1-[2-(2-[1,3]Dioxolan-2-yl-ethyl)-[1,3]dioxolan-2-yl]-2-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / p-toluenesulfonyl chloride / toluene / 11 h

2: 1.3 g / hydrazine / ethanol / 0.25 h / Heating

With p-toluenesulfonyl chloride; hydrazine; In ethanol; toluene;
DOI:10.1021/jm00186a020