(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

Base Information

Chemical Name:(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester
CAS No.:74075-32-4
Molecular Formula:C₃₁H₃₂N₂O₅
Molecular Weight:512.605
Hs Code.:

Synonyms:(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

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Chemical Property of (5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

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Technology Process of (5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

There total 16 articles about (5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 74075-31-3,83356-17-6
(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoic acid

: 74075-32-4
(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 50h;
DOI:10.1016/j.bmcl.2006.06.003

Reference yield: 85.0%

: 910316-84-6
(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-proline benzyl ester

: 98-88-4
benzoyl chloride

: 74075-32-4
(5S)-5-[(N-benzoyl)amino]-4-oxo-6-phenyl-hexanoyl-L-proline benzyl ester

Guidance literature:: (5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-proline benzyl ester; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Cooling with ice; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water;

benzoyl chloride; With pyridine; at 0 - 20 ℃; Inert atmosphere; Cooling with ice;