N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

Base Information

Chemical Name:N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide
CAS No.:1407767-72-9
Molecular Formula:C₂₄H₂₇NO₇S
Molecular Weight:473.547
Hs Code.:

Synonyms:N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

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Chemical Property of N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

There total 5 articles about N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: N-[3,4-bis(tert-butyldimethylsilyloxy)benzyl]-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

: 1407767-72-9
N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

Guidance literature:: With acetic acid; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0032-1316559

Reference yield:

: 1259425-46-1
C₁₉H₃₃NO₂Si₂

: 1407767-72-9
N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / diethyl ether / 2 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

4: acetic acid; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; acetic acid; triethylamine tris(hydrogen fluoride); triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1055/s-0032-1316559

Reference yield:

: 765962-55-8
(3,4-bis((tert-butyldimethylsilyl)-oxy)phenyl)methanamine

: 1407767-72-9
N-(3,4-dihydroxybenzyl)-4-methyl-N-(3,4,5-trimethoxybenzyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

3: acetic acid; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; acetic acid; triethylamine tris(hydrogen fluoride); triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0032-1316559