1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

Base Information

Chemical Name:1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol
CAS No.:133229-04-6
Molecular Formula:C₂₀H₂₃ClN₂O₄
Molecular Weight:390.867
Hs Code.:

Synonyms:1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

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Chemical Property of 1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

Chemical Property:

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Technology Process of 1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

There total 1 articles about 1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26905-02-2
4-(4-chlorophenyl)piperidine

: 125228-75-3
4-nitrophenyl 2-oxiranylmethyl ether

: 133229-04-6
1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

Guidance literature:: In ethanol; for 4h; Heating;
DOI:10.1021/jm00109a007

Reference yield:

: 133229-04-6
1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

: 1-(4-Amino-phenoxy)-3-[4-(4-chloro-phenyl)-piperidin-1-yl]-propan-2-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1h; under 760 Torr;
DOI:10.1021/jm00109a007

Reference yield:

: 133229-04-6
1-[4-(4-Chloro-phenyl)-piperidin-1-yl]-3-(4-nitro-phenoxy)-propan-2-ol

: 133229-26-2
N-(4-{3-[4-(4-Chloro-phenyl)-piperidin-1-yl]-2-hydroxy-propoxy}-phenyl)-methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 1 h / 760 Torr

2: dimethylformamide / 1 h / 0 °C

With hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a007