Se-phenyl 15-hydroxypentadecanecarboselenoate

Base Information

Chemical Name:Se-phenyl 15-hydroxypentadecanecarboselenoate
CAS No.:73335-23-6
Molecular Formula:C₂₁H₃₄O₂Se
Molecular Weight:397.46
Hs Code.:

Synonyms:Se-phenyl 15-hydroxypentadecanecarboselenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Se-phenyl 15-hydroxypentadecanecarboselenoate

Chemical Property:

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Technology Process of Se-phenyl 15-hydroxypentadecanecarboselenoate

There total 7 articles about Se-phenyl 15-hydroxypentadecanecarboselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 73335-21-4
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

: 73335-23-6
Se-phenyl 15-hydroxypentadecanecarboselenoate

Guidance literature:: With acetic acid; In acetone; for 24h;
DOI:10.1021/jo00321a008

Reference yield: 34.0%

: 18270-60-5
15-hydroxy-pentadecanoic acid hydrazide

: 6996-92-5
benzeneseleninic acid

: 4617-33-8
15-hydroxylpentadecanoic acid

: 73335-23-6
Se-phenyl 15-hydroxypentadecanecarboselenoate

Guidance literature:: In dichloromethane; for 24h; Yields of byproduct given;
DOI:10.1021/jo00321a008

Reference yield:

: 76529-42-5
methyl 15-hydroxypentadecanoate

: 73335-23-6
Se-phenyl 15-hydroxypentadecanecarboselenoate

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide / 31 h

2: hydrazine / ethanol / 1 h / Heating

3: 81 percent / triphenylphosphine / CH₂Cl₂ / 0.67 h

4: 100 percent / 50percent acetic acid / acetone / 24 h

With 1H-imidazole; acetic acid; triphenylphosphine; hydrazine; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo00321a008