15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Base Information

Chemical Name:15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester
CAS No.:73335-21-4
Molecular Formula:C₂₇H₄₈O₂SeSi
Molecular Weight:511.722
Hs Code.:

Synonyms:15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Suppliers and Price of 15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

There total 5 articles about 15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 6996-92-5
benzeneseleninic acid

: 73335-17-8
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecanoic acid hydrazide

: 73335-21-4
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Guidance literature:: With triphenylphosphine; In dichloromethane; for 0.666667h;
DOI:10.1021/jo00321a008

Reference yield:

: 76529-42-5
methyl 15-hydroxypentadecanoate

: 73335-21-4
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 31 h

2: hydrazine / ethanol / 1 h / Heating

3: 81 percent / triphenylphosphine / CH₂Cl₂ / 0.67 h

With 1H-imidazole; triphenylphosphine; hydrazine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00321a008

Reference yield:

: 121942-41-4
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

: 73335-21-4
15-(tert-Butyl-dimethyl-silanyloxy)-pentadecaneselenoic acid Se-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 1 h / Heating

2: 81 percent / triphenylphosphine / CH₂Cl₂ / 0.67 h

With triphenylphosphine; hydrazine; In ethanol; dichloromethane;
DOI:10.1021/jo00321a008