1--3-fluorobenzene

Base Information

• Chemical Name: 1--3-fluorobenzene
• CAS No.: 127974-67-8
• Molecular Formula: C₁₉H₁₅FS₂
• Molecular Weight: 326.459

Synonyms:1--3-fluorobenzene

Chemical Property of 1--3-fluorobenzene

Chemical Property:

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Technology Process of 1--3-fluorobenzene

There total 2 articles about 1--3-fluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-methyl-N'-(3-fluorobenzylidene)benzenesulfonohydrazide (343229-18-5) + diphenyldisulfane (882-33-7) → 1--3-fluorobenzene (127974-67-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 100 ℃;

DOI:10.1002/adsc.201600855

Reference yield: 78.0%

diphenyldisulfane (882-33-7) + 3-Fluorobenzaldehyde (456-48-4) → 1--3-fluorobenzene (127974-67-8)

Guidance literature:

With tributylphosphine; In benzene;

DOI:10.1021/jo00301a026

upstream raw materials:

diphenyldisulfane

3-Fluorobenzaldehyde

4-methyl-N'-(3-fluorobenzylidene)benzenesulfonohydrazide

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