1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

Base Information

Chemical Name:1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene
CAS No.:1533425-04-5
Molecular Formula:C₁₅H₂₁NOS₃
Molecular Weight:327.536
Hs Code.:

Synonyms:1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

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Technology Process of 1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

There total 2 articles about 1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 463-71-8
thiophosgene

: 1533425-03-4
3-tert-butylsulfanyl-5-(2-methylpropane-2-sulfinyl)phenylamine

: 1533425-04-5
1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

Guidance literature:: With calcium carbonate; In dichloromethane; water; at 0 - 20 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1533425-02-3
1-tert-butylsulfanyl-3-(2-methylpropane-2-sulfinyl)-5-nitrobenzene

: 1533425-04-5
1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride / methanol; water / 70 °C / 760.05 Torr / Inert atmosphere

2: calcium carbonate / dichloromethane; water / 0 - 20 °C / 760.05 Torr / Inert atmosphere

With iron; ammonium chloride; calcium carbonate; In methanol; dichloromethane; water;

Reference yield: 42.0%

: 420-04-2
CYANAMID

: 1533425-04-5
1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene

: 74-88-4
methyl iodide

: (Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3-tert-butylsulfanyl-5-(2-methylpropane-2-sulfinyl)phenyl)carbamimidothioate

Guidance literature:: CYANAMID; With sodium methylate; In methanol; for 0.25h; under 760.051 Torr; Inert atmosphere;

1-tert-butylsulfanyl-3-isothiocyanato-5-(2-methylpropane-2-sulfinyl)benzene; In methanol; for 1h; under 760.051 Torr; Inert atmosphere;

methyl iodide; In methanol; at 20 ℃; under 760.051 Torr; Inert atmosphere;