3-fluoro-4-nitrobenzene

Base Information

• Chemical Name: 3-fluoro-4-nitrobenzene
• CAS No.: 156078-93-2
• Molecular Formula: C₁₀H₁₃FN₂O₄
• Molecular Weight: 244.223

Synonyms:3-fluoro-4-nitrobenzene

Chemical Property of 3-fluoro-4-nitrobenzene

Chemical Property:

Purity/Quality:

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Technology Process of 3-fluoro-4-nitrobenzene

There total 1 articles about 3-fluoro-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,4-difluoronitrobenzene (369-34-6) + 2,2'-iminobis[ethanol] (111-42-2) → 3-fluoro-4-nitrobenzene (156078-93-2)

Guidance literature:

at 130 ℃; for 2h;

DOI:10.1021/jm00026a013

Reference yield: 99.0%

3-fluoro-4-nitrobenzene (156078-93-2) → 3-fluoro-4-nitrobenzene (156079-59-3)

Guidance literature:

With piperidine; thionyl chloride; In dichloromethane; for 1h; Heating;

DOI:10.1021/jm00026a013

Reference yield: 81.0%

methanesulfonyl chloride (124-63-0) + 3-fluoro-4-nitrobenzene (156078-93-2) → 3-fluoro-4-nitrobenzene (156079-59-3)

Guidance literature:

In N,N-dimethyl-formamide;

upstream raw materials:

3,4-difluoronitrobenzene

2,2'-iminobis[ethanol]

Downstream raw materials:

3-fluoro-4-nitrobenzene

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