4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

Base Information

Chemical Name:4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline
CAS No.:1288340-55-5
Molecular Formula:C₁₃H₁₀ClF₄N₃
Molecular Weight:319.689
Hs Code.:

Synonyms:4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

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Chemical Property of 4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

Chemical Property:

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Technology Process of 4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

There total 4 articles about 4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1288339-36-5
2-[4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-5-nitropyridine

: 1288340-55-5
4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

Guidance literature:: With iron; ammonium chloride; In ethanol; water; for 1h; Reflux;

Reference yield:

: 1062295-85-5,1027617-86-2
3-cyclopropyl-5-(trifluoromethyl)-1H-pyrazole

: 1288340-55-5
4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.5 h / 90 °C / Inert atmosphere

1.2: 2 h / 90 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0 - 28 °C

3.1: ammonium chloride; iron / ethanol; water / 1 h / Reflux

With N-chloro-succinimide; iron; potassium carbonate; ammonium chloride; In ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1288339-35-4
2-[5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-5-nitropyridine

: 1288340-55-5
4-(4-chloro-5-cyclopropyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)-3-fluoroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 0 - 28 °C

2: ammonium chloride; iron / ethanol; water / 1 h / Reflux

With N-chloro-succinimide; iron; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;