5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

Base Information

Chemical Name:5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene
CAS No.:1400655-54-0
Molecular Formula:C₃₄H₃₀O₆
Molecular Weight:534.609
Hs Code.:

Synonyms:5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

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Chemical Property of 5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

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Technology Process of 5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

There total 9 articles about 5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1400655-48-2
(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

: 1400655-54-0
5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

Guidance literature:: With iron(III) chloride hexahydrate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-53-9
1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

: 1400655-54-0
5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 4 h / 20 °C

2: iron(III) chloride hexahydrate / dichloromethane / 3 h / 20 °C

With iron(III) chloride hexahydrate; toluene-4-sulfonic acid; In dichloromethane; toluene;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-50-6
3,5,7-trimethoxyphenanthrene-9-carboxylic Acid

: 1400655-54-0
5-(3,5-dimethoxyphenyl)-1,3,9-trimethoxy-4-(4-methoxyphenyl)acephenanthrylene

Guidance literature:: Multi-step reaction with 5 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 25 °C

2: tetrahydrofuran / 3 h / 0 - 25 °C

3: tetrahydrofuran / 3 h / 0 - 25 °C

4: toluene-4-sulfonic acid / toluene / 4 h / 20 °C

5: iron(III) chloride hexahydrate / dichloromethane / 3 h / 20 °C

With iron(III) chloride hexahydrate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 2: |Grignard Reaction / 3: |Grignard Reaction;
DOI:10.1021/jo301345a