1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

Base Information

Chemical Name:1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol
CAS No.:1400655-53-9
Molecular Formula:C₃₄H₃₄O₇
Molecular Weight:554.64
Hs Code.:

Synonyms:1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

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Chemical Property of 1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

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Technology Process of 1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

There total 7 articles about 1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1400655-49-3
(3,5-dimethoxyphenyl)(3,5,7-trimethoxyphenanthren-9-yl)methanone

: 38769-92-5
4-methoxybenzylmagnesium chloride

: 1400655-53-9
1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

Guidance literature:: In tetrahydrofuran; at 0 - 25 ℃; for 3h;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-50-6
3,5,7-trimethoxyphenanthrene-9-carboxylic Acid

: 1400655-53-9
1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 25 °C

2: tetrahydrofuran / 3 h / 0 - 25 °C

3: tetrahydrofuran / 3 h / 0 - 25 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Grignard Reaction / 3: |Grignard Reaction;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-51-7
3,5,7-trimethoxyphenanthrene-9-carbonitrile

: 1400655-53-9
1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 2-methoxy-ethanol; water; sodium hydroxide / 18 h / 150 °C

2: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 25 °C

3: tetrahydrofuran / 3 h / 0 - 25 °C

4: tetrahydrofuran / 3 h / 0 - 25 °C

With 2-methoxy-ethanol; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; 3: |Grignard Reaction / 4: |Grignard Reaction;
DOI:10.1021/jo301345a