(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

Base Information

Chemical Name:(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene
CAS No.:1400655-48-2
Molecular Formula:C₃₄H₃₂O₆
Molecular Weight:536.624
Hs Code.:

Synonyms:(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

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Chemical Property of (E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

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Technology Process of (E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

There total 8 articles about (E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1400655-53-9
1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(3,5,7-trimethoxyphenanthren-9-yl)ethanol

: 1400655-48-2
(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

: 1400655-58-4
(Z)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 20 ℃; for 4h;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-51-7
3,5,7-trimethoxyphenanthrene-9-carbonitrile

: 1400655-48-2
(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

: 1400655-58-4
(Z)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

Guidance literature:: Multi-step reaction with 5 steps

1: 2-methoxy-ethanol; water; sodium hydroxide / 18 h / 150 °C

2: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 25 °C

3: tetrahydrofuran / 3 h / 0 - 25 °C

4: tetrahydrofuran / 3 h / 0 - 25 °C

5: toluene-4-sulfonic acid / toluene / 4 h / 20 °C

With 2-methoxy-ethanol; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 3: |Grignard Reaction / 4: |Grignard Reaction;
DOI:10.1021/jo301345a

Reference yield:

: 1400655-50-6
3,5,7-trimethoxyphenanthrene-9-carboxylic Acid

: 1400655-48-2
(E)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

: 1400655-58-4
(Z)-10-(1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)vinyl)-2,4,6-trimethoxyphenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 25 °C

2: tetrahydrofuran / 3 h / 0 - 25 °C

3: tetrahydrofuran / 3 h / 0 - 25 °C

4: toluene-4-sulfonic acid / toluene / 4 h / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2: |Grignard Reaction / 3: |Grignard Reaction;
DOI:10.1021/jo301345a